Overview
Ultrasonic and microwave combined reaction system (model: HX-CW1000) has the functions of microwave, ultrasonic, microwave and ultrasonic separate control and coordination. The system also realizes the functions of 7-inch touch interface control, data storage and high definition visualization real-time display of reaction status. The product is widely used in chemical synthesis in universities, scientific research institutes, biology, materials industry and mining and many other fields. The basic principles of microwave, ultrasonic, ultraviolet light and other basic principles have effective catalysis for reactants, which can create a variety of synthesis conditions and speed up chemical synthesis reactions.
Features
1. The temperature control system uses a Platinum Electric Group Sensor to ensure accurate temperature control.
2. The container capacity is 1000ml, suitable for a variety of reaction requirements.
3. Operating system adopts microcomputer control technology and supports multi-stage program control mode.
4. Ultrasonic Power 1800W can be fine-tuned, Frequency 20KHz, Ultrasonic Probe can intervene in or non-invasive samples, acting on samples through cavitation effect or air transmission.
5. Standard ultrasonic Probe diameter φ 20, suitable for reaction vessels of different diameters.
6. Microwave Frequency 2450MHz, Non-Pulse Continuous Automatic Frequency Conversion Control, Power 0-100% Automatic Continuous Adjustable.
7. Industrial magnetron, Maximum output power 1000W.
8. UV catalytic system wavelength 253.7nm, Power 100W.
9. The stirringdevice is magnetic stirring, and the Rotation speed is adjustable from 0 to 2500rpm.
10. Multifunctional operation mode, can be extended to microwave extraction, microwave synthesis, ultrasonic wall breaking, etc.
11. Six-story steel structure safety furnace door, using buffer floating design to ensure experimental safety.
12. The mechanical lock and the electronic lock cooperate to automatically cut off the microwave when the furnace door is abnormally opened.
13. The furnace cavity is integrally formed with 316L industrial grade stainless steel, lame plating 6 layers of PFA anti-corrosion coating.
14. Microcomputer control technology, support historical data viewing, data export and import.
15. Capacitive LCD touch screen, real-time display of temperature, Heating time, thermostatic time, Microwave Power, reaction process.
16. The instrument has a built-in method library that can store 200 methods.
17. The reactor can be optionally equipped with PTFE or high temperature and corrosion resistant Glass material, with a volume of 1000ml.
18. Glass conduit can be connected to the reactor to support the open reaction system, and drop funnel and condenser can be installed for reflux reaction.
Principle
The ultrasonic-microwave combined reaction system uses basic principles such as microwave, ultrasonic, and ultraviolet light to catalysis the reactants. Microwaves generate high-frequency electromagnetic waves to accelerate molecular motion through non-pulsed continuous automatic frequency conversion control; ultrasonic waves generate mechanical vibrations to promote the reaction through cavitation effect or air transmission; ultraviolet light provides photocatalytic conditions. These energy synergies can create a variety of synthesis conditions and speed up the chemical synthesis reaction process.
Applications
Universities, research institutes, biology, materials industry and mining
Steps
Select reactor materials (such as PTFE or High Temperature Glass) to ensure that the volume is 1000ml.
2. Connect Glass conduit, drop funnel or condenser tube, set up open reaction system.
3. Select the operation mode (microwave, ultrasonic or cooperative) through the 7-inch touch capacitive screen, and call the built-in method library or custom parameters.
4. Set parameters such as Microwave Power (0-100% adjustable), Ultrasonic Power (1800W fine-tunable), Temperature (0-350 ℃), Pressure (0-15Mpa), Stirring Rotation speed (0-2500rpm).
5. Start the system to monitor temperature, Heating time, thermostatic time, Microwave Power and reaction process in real time.
6. After the experiment, review the historical data or export the data for subsequent analysis.
Notice
Make sure the furnace door is fully closed, and the mechanical lock and electronic lock are coordinated to prevent the furnace door from opening during operation.
When the furnace door is abnormally opened, the instrument will automatically cut off the microwave and stop working. It needs to be checked before starting.
- Check whether the reactor material is resistant to high temperature and corrosion before use to avoid damage.
- Pay attention to the interventional or non-interventional mode of ultrasonic Probe during operation, and choose according to the characteristics of the sample.
- Avoid overheating and overpressure operation, Temperature range 0-350 ℃, pressure range 0-15Mpa.
- Regularly check the furnace cavity anticorrosive coatings and Sensors to ensure long-term stable operation of the equipment.
Make sure there is sufficient storage space before data export to avoid data loss.
